Clean ¹³⁸La

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GigaBecquerel
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Clean ¹³⁸La

Post by GigaBecquerel » 06 Nov 2021, 01:42

Hello guys!

Lanthanum often tends to be contaminated with actinium, as you can see here:
viewtopic.php?f=5&t=900

I got my hands on ~150 g of LaCl3 (at least that's what it's labled as, but one of the powders is not hygroscopic at all, so I have no idea what I actually got), and so I took a spectrum of it.
The samples were left in their containes and just propped up on my NaI, inside the lead castle.
photo_2021-11-04_21-12-36.jpg
photo_2021-11-04_21-12-36.jpg (93.58 KiB) Viewed 2736 times
photo_2021-11-04_21-12-36 (2).jpg
photo_2021-11-04_21-12-36 (2).jpg (70.16 KiB) Viewed 2736 times
After around 13 hours I took the samples out of my lead castle and proceeded to take around 5 hours of background.
Subtracting the background (scaled accordingly) from the actual spectrum showed all three ¹³⁸La peaks nicely and was clear of any actinium contamination!
Raw Spectrum with background included
Raw Spectrum with background included
Clean Spectrum
Clean Spectrum
Please note that the total activity was 30-50 Bq, so a longer sample time would have improved the spectrum a lot.
Lanthanum is a nice sample to test the low end of your detectors sensitivity, the metal is ~0.8 Bq/g, and you'll end up with a gamma every two seconds or thereabout.

Lukas

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Peter-1
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Re: Clean ¹³⁸La

Post by Peter-1 » 08 Nov 2021, 01:08

I also measured La138 a few months ago. It was 100 grams of La oxide. I could only see the 2 lines of La138.
2021_02_07-Lanthanoxid.png
Peter

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