When we want to measure x-rays we are only interested in the low energy photons especially those under 100 keV. We could use a typical 1.5 x 1.5" NaI(Tl) detector, but such a probe will also count gamma rays up to 3 MeV, which means the region of interest is only 3% of the spectrum.
The solution is to use a thin crystal, a 1 mm slither of NaI(Tl) will stop 100 keV x-rays while most of the the higher energy gamma will pass right through.
One of the problems we face when building such an x-ray detector is the attenuation factor of the aluminium housing, even a thin 0.5 mm layer of aluminium can attenuate the low energy x-rays we are interested in, so if we make a detector with an encapsulated 1 mm NaI(Tl) crystal the region below 20 keV may not be visible.
One solution to this problem is to use a detector with a Beryllium (Be) window, these are commercially available and quite expensive, and building one means working with Be which is quite carcinogenic if inhaled.
So I asked my crystal supplier if they could provide a thin slice of CsI(Tl), the benefit of using CsI(Tl) is that it is much less hygroscopic and does not need to be encapsulated. The polished crystal mounts straight to the PMT with a thin backing of white PTFE (Teflon) and some thin black plastic to block out light. The thin layer of plastic should be relatively transparent to x-rays, compared to Aluminium.
While CsI(Tl) is about twice the price of NaI(Tl), a thin 2 mm slice as the one I am holding in the picture below, is very affordable.
I am waiting for some PTFE to arrive before assembling and testing this probe, it will be a 2.0" x 0.1" GS-2001-CSI
Will post below once I have built and tested this one.
Steven
* References taken from Saint Gobain - Efficiency Calculations for Selected Scintillators
Building an XRF detector with CsI(Tl)
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Building an XRF detector with CsI(Tl)
Steven Sesselmann | Sydney | Australia | https://gammaspectacular.com | https://beejewel.com.au | https://www.researchgate.net/profile/Steven-Sesselmann
Re: Building an XRF detector with CsI(Tl)
Hi Steven,
Yes, a thin slice of CsI(Tl) can be used as xrf detector best example is the Rap-47 detector.
It is simple to build a detector like that, only the tricky part is you will need a good pmt that has a low noise level that is not always easy to find.
Simple and cheap aluminum house hold foil can be used as the entrance window.
I made a few detectors like that before some years ago and still have some slices CsI(Tl) from the test that I did, the lowest detectable energy will be around 10KeV although resolution is not very good at the lowest energies.
Have to look if I still have some test somewhere if I find them I shall post them here.
Luuk
Yes, a thin slice of CsI(Tl) can be used as xrf detector best example is the Rap-47 detector.
It is simple to build a detector like that, only the tricky part is you will need a good pmt that has a low noise level that is not always easy to find.
Simple and cheap aluminum house hold foil can be used as the entrance window.
I made a few detectors like that before some years ago and still have some slices CsI(Tl) from the test that I did, the lowest detectable energy will be around 10KeV although resolution is not very good at the lowest energies.
Have to look if I still have some test somewhere if I find them I shall post them here.
Luuk
Re: Building an XRF detector with CsI(Tl)
Can't wait to see the spectra once you've finished this detector. Hope you'll post a price to make more if it works!
Christopher Lloyd
Salt Lake City, Utah (US)
Setup: Modified GS-STANDUP-20 with GS-USB-PRO
Primary Detector: GS 2" x 2" CsI(Tl)
Salt Lake City, Utah (US)
Setup: Modified GS-STANDUP-20 with GS-USB-PRO
Primary Detector: GS 2" x 2" CsI(Tl)
Re: Building an XRF detector with CsI(Tl)
Were you able to locate any of your test results? I am interested in CsI(Tl) for low energy detection (<100KeV), and I'm curious what performance you obtained (particularly interested in thickness).luuk wrote: ↑06 Jan 2020, 06:47Hi Steven,
Yes, a thin slice of CsI(Tl) can be used as xrf detector best example is the Rap-47 detector.
It is simple to build a detector like that, only the tricky part is you will need a good pmt that has a low noise level that is not always easy to find.
Simple and cheap aluminum house hold foil can be used as the entrance window.
I made a few detectors like that before some years ago and still have some slices CsI(Tl) from the test that I did, the lowest detectable energy will be around 10KeV although resolution is not very good at the lowest energies.
Have to look if I still have some test somewhere if I find them I shall post them here.
Luuk
Regarding the selection of PMT, what are some examples of suitable models?
Re: Building an XRF detector with CsI(Tl)
I did a quick test with a home made leg detector.
interested please read the pdf.
Luuk
interested please read the pdf.
Luuk
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Re: Building an XRF detector with CsI(Tl)
Nice Luuk. Thanks for sharing.
Cheers, Tom Hall / IRAD INC / Stuart, FL USA
Please check out my eBay Store: http://stores.ebay.com/The-Rad-Lab
Please check out my eBay Store: http://stores.ebay.com/The-Rad-Lab
Re: Building an XRF detector with CsI(Tl)
Few years ago I bought two of these Soviet-crystals:
very thin NaI(Tl) covered with beryllium window.
Sometimes they still appears on ebay.
They have some yellow spot but resolution is decent.
I made a good low energy probe, nice for xrf experiments.
very thin NaI(Tl) covered with beryllium window.
Sometimes they still appears on ebay.
They have some yellow spot but resolution is decent.
I made a good low energy probe, nice for xrf experiments.
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